A robust pulse sequence for the determination of small homonuclear dipolar couplings in magic-angle spinning NMR
We present a new solid-state NMR pulse sequence that accomplishes efficient broad-band dipolar recoupling in systems with small dipolar couplings and large chemical shift anisotropies. The method involves a supercycled symmetry-based recoupling sequence incorporated in a constant-interval data acqui...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
| Published: |
2004-05-21.
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| Subjects: | |
| Online Access: | Get fulltext |